抗氧化剂1076高效液相色谱法的改进研究  

High performance liquid chromatography analysis of antioxidant 1076

作　　者：皇甫慧君[1] 任蕊[1] 宋扬扬[1] 王军[1] 党璐[1] 

机构地区：[1]陕西省石油化工研究设计院,陕西西安710054

出　　处：《应用化工》2013年第7期1339-1340,1343,共3页Applied Chemical Industry

基　　金：陕西省科技攻关计划项目(2009K01-42)

摘　　要：采用高效液相色谱分析抗氧化剂1076,并与HG/T 3795—2005中抗氧化剂1076的分析方法进行了比较。结果表明,采用甲醇/乙酸乙酯(V/V=50∶50)作流动相,紫外检测器,275 nm波长下,在0.5～2.5 mg/mL具有较好的线性,标准偏差为0.000 4,平均质量回收率100.2%,出峰时间提前,提高了分析效率。The analyzing antioxidants 1076 by high performance liquid chromatography was carried out and comparied with the method of HG/T 3795—2005.Results showed that methanol/ethyl acetate（V/V=50∶ 50） was used as mobile phase,UV-detector is used in 275 nm wavelength,the linear range is between the concentration 0.5~2.5 mg/mL,the standard deviation is 0.000 4 and the average mass recovery is 100.2%.Chromatographic peak time is shortened and analysis efficiency is improved.

关 键 词：高效液相色谱 抗氧化剂1076 改进 

分 类 号：TQ075[化学工程]