几种常见中成药中有机磷农药残留检测分析  

The analysis of the remains of organopho-sphorus in several Chinese mediesines

作　　者：刘晓霞[1] 高洁[2] 

机构地区：[1]天津中医药大学第一附属医院,天津300193 [2]天津市人民医院,天津300120

出　　处：《天津中医药》2013年第7期436-438,共3页Tianjin Journal of Traditional Chinese Medicine

摘　　要：旧的】建立几种中成药中有机磷农药残留量的测定方法。【方法】采用气相色谱法（GC法），氢火焰离子化（FID）检测器，对精致银翘解毒片、桑菊感冒片、羚羊感冒片、通宣理肺片、清瘟解毒片等几种中成药中有机磷类农药的残留量进行测定。【结果】5种中成药中未检出有机磷农药残留，平均回收率在63．3％。79．7％之间，RSD在5．2％～12．5％之间。【结论】5种中成药中有机磷农药残留未见检出，说明中成药中一般不含有机磷类农药或者含量极低，因此为安全、放心的使用中成药提供了科学依据，并且为检测中成药中有机磷农药残留提供了可行的测定方法。[Objective] To determine the remains of organophosphorus in several Chinese medicines. [Methods] The remains of organophosphorus in Jingzhi Yinqiao jiedu tablets Sangju ganmao tablets, Lingyang ganmao tablets, Tongxuan lifei tablets and Qingwen jiedu tablets were determined by GC with FID.[Results] The five kinds of Chinese medicines were not detected orgauophosphorus pesti- cide residues.The average reeoweries and RSD of the method were 63.3%-79.7%and 5.2%-12.5%. [Conclusion] No detectable residues of organophosphorus pesticides in 5 kinds of Chinese medicine. Description in traditional Chinese medicine generally do not contain organic phosphorus pesticide or very low content. It provides a scientific basis for the use of proprietary Chinese medicines safety and rest assured. And for the determination of organophosphorus pesticide residues in traditional Chinese medicine provides a method for the de-termination of feasible.

关 键 词：中成药 有机磷 气相色谱 

分 类 号：R284.1[医药卫生—中药学]