皱皮柑果皮中总黄酮的回流提取工艺研究  

Refluxing extraction technology of total flavonoids from the peel of rough-peel mandarin

作　　者：张珉[1] 李良导[2] 钟晓红[2] 孙化鹏[2] 王超华[3] 

机构地区：[1]湖南省林业科学院,湖南长沙410004 [2]湖南农业大学,湖南长沙410128 [3]广州大学,广东广州510006

出　　处：《湖南林业科技》2013年第4期14-17,共4页Hunan Forestry Science & Technology

基　　金：湖南省科学技术厅项目(BK0660)

摘　　要：采用回流提取法,通过单因素试验和正交试验,研究了皱皮柑果皮中总黄酮的提取工艺。结果表明:皱皮柑果皮中总黄酮的最佳提取工艺条件为乙醇浓度70%、水浴温度90℃、料液比1∶30、回流时间60 min、粒径为20目(0.90 mm)。在此条件下,总黄酮提取率可达1.56%。各因素对总黄酮提取率影响的主次顺序为回流时间>粒径>水浴温度>乙醇浓度>料液比。The extraction technology of total flavonoids from the peel of rough-peel mandarin by refluxing method was studied through the single-factor and orthogonal experiments. The results showed that, the optimal extraction conditions were ethanol concentration 70%, water bath temperature 90℃, ratio of material to solvent 1 ： 30, refluxing time of 60 min and particle size 20 meshes. At the optimal conditions, the extraction rate of total flavonoids reached 1.56%. The sequences Qf factors influencing the extraction rate were refluxing time 〉 particle size 〉 water bath temperature 〉 ethanol concentration 〉 the ratio of material to solvent.

关 键 词：皱皮柑 总黄酮 回流提取 提取工艺 

分 类 号：R284[医药卫生—中药学]