糠醛缩氨基硫脲合Cu配合物的制备与表征  

Synthesis and Characterization of Furaldehyde-thiosemicarbazide Complex with Copper(Ⅱ)

作　　者：孟祥福[1] 

机构地区：[1]承德石油高等专科学校 化工系,河北承德067000

出　　处：《化学世界》2013年第9期554-556,共3页Chemical World

摘　　要：以糠醛和氨基硫脲为原料,冰醋酸为催化剂,制备了希夫碱,用该希夫碱与醋酸铜合成了配合物,用红外光谱和紫外光谱对其结构进行了表征。同时测定了希夫碱及配合物熔点、测试其溶解性,讨论了影响希夫碱产率的因素。Furaldehyde-thiosemicarbazide was synthesized from furaldehyde and thiosemicarbazide with HAc as catalyst, and then its copper complex was synthesized. The melting points of the compounds were determined and their solubility was tested. Their structures were characterized by UV and IR spectroscopy. The factors influencing the yield were discussed.

关 键 词：糠醛 氨基硫脲 希夫碱 金属配合物 

分 类 号：O627.23[理学—有机化学]