流动注射-在线蒸馏法同时测定水样中挥发酚及氰化物  

Simultaneous Determination of Volatile phenol and Cyanide in Environment Water by Flow Injection-On Line Distillation Analysis

作　　者：罗建民 张静 殷新 

机构地区：[1]新疆维吾尔自治区分析测试研究院检测中心,乌鲁木齐市科学北路374号830011

出　　处：《光谱实验室》2013年第5期2525-2528,共4页Chinese Journal of Spectroscopy Laboratory

基　　金：新疆维吾尔自治区科研院所改革与发展专项资金项目(20100024);新疆维吾尔自治区公益性科研究院基本科研业务专项经费项目(KY2012128)

摘　　要：采用流动注射在线蒸馏法同时测定了水样中挥发酚及氰化物。结果表明:其线性范围在0—100Lg/L时,均具有良好的线性关系,挥发酚和氰化物的方法检出限分别为1.2Lg/L和1.0Lg/L,精密度RSD均小于3%,挥发酚和氰化物平均回收率分别为90.6%和93.4%。The method of simultaneous determination of volatile phenol and cyanide in water by flow injection-on line distillation analysis is illustrated. The calibration graphs obtained by the method are linear up to 100μg/L of volatile phenolics and cyanide, the detection limit of volatile phenol and cyanide are 1. 2μg/L and 1. 0 μg/L respectively. RSD is less than 3%, The recoveries of volatile phenol and cyanide are 90. 6% and 93.4% respectively.

关 键 词：流动注射 在线蒸馏 环境水样 挥发酚 氰化物 

分 类 号：O657.32[理学—分析化学]