甲基三乙氧基硅烷的制备工艺研究  

Study on the Preparation of Methyltriethoxysilane

作　　者：许健[1] 陈利民[1] 郑战江[1] 蒋剑雄[1] 来国桥[1] 

机构地区：[1]杭州师范大学有机硅化学及材料技术教育部重点实验室,浙江杭州310012

出　　处：《杭州师范大学学报（自然科学版）》2013年第4期301-303,共3页Journal of Hangzhou Normal University(Natural Science Edition)

基　　金：钱江人才项目(2010R0017)

摘　　要：详细研究了甲基三氯硅烷的醇解工艺,通过考察原料配比、溶剂效应、温度效应以及N2的鼓泡速度对反应收率的影响,开发出高效合成甲基三乙氧基硅烷的工艺,收率高达84%.The paper studied the alcoholysis of methyl trichlorosilane in detail, investigated the effects of different variables such as the ratio of raw materials, solvent, temperature and the bubbled speed of N2 on the reaction, and finally developed an efficient technology for the preparation of methyltriethoxysilane with high yield which was up to 84 %.

关 键 词：甲基三氯硅烷 甲基三乙氧基硅烷 醇解反应 

分 类 号：O627.4[理学—有机化学]