Synthesis, Characterization and X-ray Crystal Structure of O,O~ˊ-Dipropyl α-（2,4-Dichlorolphenoxyacylamido）-α-（4-methoxyphenyl） Methylphosphonates  

作　　者：宁丽红 彭浩 贺红武 

机构地区：[1]Key Laboratory of Pesticide and Chemical Biology, Ministry of Education and College of Chemistry, Central China Normal University [2]College of Science, Huazhong Agricultural University

出　　处：《Chinese Journal of Structural Chemistry》2013年第9期1392-1396,共5页结构化学（英文）

基　　金：supported by the National Basic Research Program of China(2010CB126100)

摘　　要：A new crystal of O,Oˊ-dipropyl-α-（2,4-dichlorolphenoxyacylamido）-α-（4-methoxyphenyl） methylphosphonates has been prepared at room temperature and characterized by elemental analysis and IR,MS,1H NMR spectra,13C NMR spectra and X-ray single-crystal determination.The complex crystallizes in triclinic,space group P1 with a = 7.858（2）,b = 12.621（4）,c = 12.621（4）,α = 96.17（3）,β = 90.960（3）,γ = 90.960（3）°,V = 1243.9（7）3,Dc = 1.346 Mg/m3,Z = 2,μ = 0.362 mm-1and F（000） = 528.A new crystal of O,Oˊ-dipropyl-α-（2,4-dichlorolphenoxyacylamido）-α-（4-methoxyphenyl） methylphosphonates has been prepared at room temperature and characterized by elemental analysis and IR,MS,1H NMR spectra,13C NMR spectra and X-ray single-crystal determination.The complex crystallizes in triclinic,space group P1 with a = 7.858（2）,b = 12.621（4）,c = 12.621（4）,α = 96.17（3）,β = 90.960（3）,γ = 90.960（3）°,V = 1243.9（7）3,Dc = 1.346 Mg/m3,Z = 2,μ = 0.362 mm-1and F（000） = 528.

关 键 词：X-ray crystallography PHOSPHONATE 

分 类 号：O73[理学—晶体学]