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机构地区:[1]浙江大学医学院附属妇产科医院,浙江杭州310006
出 处:《中国中药杂志》2013年第20期3525-3527,共3页China Journal of Chinese Materia Medica
摘 要:研究马肾果叶的化学成分。采用硅胶、Sephadex LH-20、高效制备液相等方法,对马肾果甲醇提取物进行分离纯化,通过质谱(MS)、波谱数据分析(1H-,13C-NMR)进行结构鉴定。从马肾果甲醇提取物中分离7个化合物,分别鉴定为dasyclamide(1),aglamide A(2),aglamide B(3),aglamide C(4),aglamide D(5),aglaroxin A 1-O-acetate(6),3'-methoxyaglaroxin A1-O-acetate(7)。上述化合物均为首次从该植物中分离得到。To study the chemical constituents from the leaves of Aglaia testicularis. The methanol extract was isolated and puri- fied by silica gel, Sephadex LH-20 and preparative HPLC. Their chemical structures were elucidated by MS and spectral data( ' H, ,3 C-NMR). Seven compounds were isolated from the leaves and identified as dasyclamide ( 1 ), aglamide A (2), aglamide B (3), aglamide C(4), aglamide D(5), aglaroxin A 1-O-acetate(6), and 3'-methoxyaglaroxin A 1-O-acetate(7). All compounds were isola- ted from this plant for the first time.
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