4,4’-二硝基二苯乙烷(烯)的合成  

Synthesis of 4,4'-Dinitrodibenzyl and 4,4'-Dinitrostilbene

作　　者：卢俊瑞[1] 王亚林 冯燕 顾玲 

机构地区：[1]天津理工学院化工系,天津300191 [2]天津职工化工学院

出　　处：《应用化学》2000年第6期651-653,共3页Chinese Journal of Applied Chemistry

基　　金：天津市 2 1世纪青年科学基金资助项目!(97370 16 11)

摘　　要：The title compounds were synthesized by oxidative dimerization of p-nitrotoluene. The effects of solvents, bases and oxidizing agents on the dimerization were investigated. The results showed that by selecting appropriate solvents, oxidizing agents, base catalysts and controlling technical conditions the yields of dinitrodibenzyl and dinitrostilbene could be reached 89.4% and 74.6%, respectively.The title compounds were synthesized by oxidative dimerization of p-nitrotoluene. The effects of solvents, bases and oxidizing agents on the dimerization were investigated. The results showed that by selecting appropriate solvents, oxidizing agents, base catalysts and controlling technical conditions the yields of dinitrodibenzyl and dinitrostilbene could be reached 89.4% and 74.6%, respectively.

关 键 词：二硝基二苯乙烯 二硝基二苯乙烯 合成 

分 类 号：O625.611[理学—有机化学]