(±)-1-[(2-羟基-5-甲基苯基)(苯基)甲基]-2-吡啶苯并咪唑的合成及晶体结构  

Synthesis and Crystal Structure of (±)-1-[(2-Hydroxy-5-methylphenyl) (phenyl)methyl]-2-pyridylbenzimidazole

作　　者：王进义[1] 周晶 程东亮[1] 菅盘铭[2] 

机构地区：[1]兰州大学化学系,兰州730000 [2]扬州大学化学系,扬州225002

出　　处：《高等学校化学学报》2000年第12期1861-1863,共3页Chemical Journal of Chinese Universities

基　　金：国家自然科学基金! (批准号 :2 9772 0 10 )资助

摘　　要：Hydroxy 5 methylphenyl)(phenyl)methyl] 2 pyridylbenzimidazole was synthesized and its crystal structure was determined by X ray four cycle diffraction method. The crystal belongs to monoclinic, space group P2 1 /c , with the crystal cell parameters: a =1.351 4(5) nm, b =0.965 9(6) nm, c =1.674 0(3) nm, β =110.2 7(2)°, V =2.049 7(14) nm 3, Z=4, D c=1.269 g/cm 3, R 1= 0.057 5 . The analyses of crystal structure show that the chain structure is formed by intermolecular H bond. [WT5HZ]Hydroxy 5 methylphenyl)(phenyl)methyl] 2 pyridylbenzimidazole was synthesized and its crystal structure was determined by X ray four cycle diffraction method. The crystal belongs to monoclinic, space group P2 1 /c , with the crystal cell parameters: a =1.351 4(5) nm, b =0.965 9(6) nm, c =1.674 0(3) nm, β =110.2 7(2)°, V =2.049 7(14) nm 3, Z=4, D c=1.269 g/cm 3, R 1= 0.057 5 . The analyses of crystal structure show that the chain structure is formed by intermolecular H bond. [WT5HZ]

关 键 词：合成 晶体结构 苯并咪唑化合物 双称子双西佛碱 

分 类 号：O626.23[理学—有机化学]