超临界流体色谱同时测定厚朴中厚朴酚和和厚朴酚(英文)  被引量:6

Simultaneous Determination of Honokiol and Magnolol in Magnoliae officinalis by Supercritical Fluid Chromatography

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作  者:邓亮[1] 郭亚东[1] 杨敏[2] 沈志强[1] 徐文秀[1] 

机构地区:[1]昆明医科大学药学院暨云南省天然药物药理重点实验室,昆明650500 [2]大理学院药学与化学学院,大理671000

出  处:《天然产物研究与开发》2013年第12期1696-1698,1708,共4页Natural Product Research and Development

基  金:National Natural Science Foundation of China(81160401);Open Research Foundation of Yunnan Key Laboratory of Pharmacology for Natural Products(No.2013G004)

摘  要:本文采用超临界流体色谱(SFC)简便快速地测定厚朴中的厚朴酚及和厚朴酚,样品经微波提取后用SFC分析,分析时间只需要20 min并且样品无需前处理,该方法可以用于厚朴中的厚朴酚及和厚朴酚的含量测定。In this study, a simple, rapid and reliable supercritical fluid chromatography (SFC) method was developed for the determination of honokiol and magnolol in Magnoliae offinalis. The sample was extracted with microwave and ana- lyzed by SFC. The whole analysis was completed within 20 min and did not need time-consuming sample preprocess. The method presented here was useful for the determination of honokiol and magnolol in M. o ff'winal.

关 键 词:厚朴 厚朴酚 和厚朴酚 超临界流体色谱 

分 类 号:R917[医药卫生—药物分析学]

 

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