纳米α-Fe_2O_3制备工艺的研究  

Study on Fabrication of Nano α-Fe_2O_3

作　　者：余鸿[1] 李敏娇[1] 张述林 司玉军[1] 曾微微[1] 

机构地区：[1]四川理工学院化学与制药工程学院,四川自贡643000 [2]材料腐蚀与防护四川省重点实验室,四川自贡643000

出　　处：《四川理工学院学报（自然科学版）》2013年第6期18-22,共5页Journal of Sichuan University of Science & Engineering(Natural Science Edition)

基　　金：绿色催化四川省高校重点实验室资助项目(LYJ03;LYJ1203)

摘　　要：用微乳液法制备纳米α-Fe2O3,研究不同反应温度和煅烧温度对其晶型结构和形貌的影响,并用X射线衍射仪(XRD)对其进行表征、用扫描电子显微镜(SEM)观察其形貌。结果表明,当煅烧温度大于600℃时,所得样品均为α-Fe2O3,随着反应温度和煅烧温度的增加,α-Fe2O3粒子的粒径逐渐增大,表面呈现蓬松多孔状,而且出现少量团聚现象。α-Fe2O3 is prepared by micro-lacteous method and characterized by X-ray diffraction （XRD） and observed by scanning electron microscopy （ SEM）. The effects of reaction and calcining temperature on the crystal structure and morphology of α-Fe2O3 are studied. The results show that the samples obtained are α-Fe2O3 when the calcining temperature is higher than 600℃, the size of particles increases as the reaction and calcining temperature increasing, the surface is porous and puffy with a small amount of agglomerations.

关 键 词：纳米材料 微乳液 纳米Α-FE2O3 

分 类 号：TB3[一般工业技术—材料科学与工程]