五松肿痛酊提高质量标准研究  

Study on Quality Standard for Wu-song Zhong-tong Tincture

作　　者：饶伟源[1] 兰保强[1] 邓聿胤[1] 吴超伟[1] 

机构地区：[1]广西中医药研究院,广西中药质量标准研究重点实验室,广西南宁530022

出　　处：《中医药导报》2013年第12期101-103,共3页Guiding Journal of Traditional Chinese Medicine and Pharmacy

基　　金：广西科技攻关项目(桂科攻1140001-35)

摘　　要：目的:对五松肿痛酊的质量标准进行修订提高。方法:采用TLC法对制剂中的买麻藤、红花、土木香、五味藤、干姜进行定性鉴别,采用HPLC法对制剂中的氯化两面针碱进行含量测定。结果:TLC法可检出买麻藤、红花、土木香、五味藤、干姜,氯化两面针碱在0.098-1.225μg范围内线性关系良好,相关系数r=0.9999,平均回收率为98.67%。(RSD%=1.32%)。结论:本法简便,快速,重复性好,可作为本品的质量控制指标。Objective：To improve the quality standard for Wu-song Zhong-tong Tincture.Methods：Gaulis gneti,Flos carthami,Radix inulae,Herba securidacae and Rhizoma Zingiberis were indentified by TLC in Wu-song Zhong-tong Tincture.And the content of Nitidine Chloride in the tincture was determined by HPLC.Results：Gaulis gneti,Flos carthami,Radix inulae,Herba securidacae and Rhizoma Zingiberis were detected by the method of TLC,and the linear range of nitidine chloride was 0.098-1.225 μg（r=0.9999）; The average recovery rate was 98.67％,（RSD=1.32％）.Conclusion：This developed method was simple,quick with good reproducibility for the quality control of Wu-song Zhong-tong Tincture.

关 键 词：五松肿痛酊 TCL法 氯化两面针碱 HPLC法 

分 类 号：R284.1[医药卫生—中药学]