马来酰肼的残留测定及其对白术品质影响的研究  

Determination of Maleic Hydrazide Residues and Its Influence on the Quality of Atractylodes macrocephala

作　　者：王春荣[1] 郑丹萍[1] 蒋鹏[1] 吴剑锋 刘影坤 田薇[1] 

机构地区：[1]浙江农林大学亚热带森林培育国家重点实验室培育基地,浙江临安311300 [2]浙江丽水市中药材产业发展中心,浙江丽水323050

出　　处：《中药材》2013年第11期1743-1747,共5页Journal of Chinese Medicinal Materials

基　　金：浙江省自然科学基金项目(LY13C140006);浙江农林大学研究生科研创新项目(3122013240149);浙江省大学生新苗人才计划(2013R412005);浙江农林大学创新创业训练计划(201202017)

摘　　要：目的:测定马来酰肼(MH)残留量,并探讨其对白术质量的影响。方法:白术现蕾期,施用不同浓度MH水剂,采收期测定白术MH残留及糖类、内酯类成分的含量,并采用独立样本t检验和主成分分析法评价MH对白术内在质量的影响。结果:白术根茎MH残留量为0.3~2.2 mg/kg;独立样本t检验显示内酯类成分的含量随MH施用浓度升高呈低-高-低趋势;主成分分析显示,施用MH对白术内在质量具有显著影响,75和100倍液时白术质量综合评价指数最高。结论:保证低残留的同时,施用适当浓度的MH可以提高白术产量及内在质量。Abstract Objective ：To determine maleie hydrazide（MH） residues and discuss its influence on the quality of Atractylodes macro- cephala. Methods ： At the bud stage, A. rru^rocephala different concentration of MH. Then MH residues, the contents of sugar and lae- tone were determined by HPLC and UV. The quality of A. macrocephala was comprehensively evaluated by independent sample t test and principal component analysis. Results ： The range of MH residues was 0. 3 - 2. 2 mg/kg. The results of independent sample t test revealed that the trend of the contents of laetone was low-high-low with the increase of MH, and the effect of MH on the content of sugar was barely obvious. Meanwhile, principal component analysis showed that comprehensive evaluation on the quality of A. macrocephala was the best when MH with 75 or 100 times water was applied. Conclusion：Proper concentration MH is applied to ensure low concen- tration MH residues and improve yield and quality of A. macrocephala.

关 键 词：白术 马来酰肼残留 糖类 内酯类 

分 类 号：R282.6[医药卫生—中药学]