经血宁颗粒的质量控制标准物质的筛选  

Screening standard quality control substance from JingXueNing granules

作　　者：许子竞 唐艳秀[2] 庞国 

机构地区：[1]广西金秀圣堂药业有限责任公司,广西金秀545700 [2]广西大学化学化工学院,广西南宁530006

出　　处：《大众科技》2014年第2期66-67,79,共3页Popular Science & Technology

摘　　要：以经血宁颗粒配伍之一的白背叶为原料,经分离纯化得化合物Ⅰ,通过定性鉴定为黄酮苷类;HPLC检测为单一纯化合物;MS测定化其分子量为564;1H NMR和13C NMR数据分析与Corymboside一致,为伞房决明苷,故以化合物Ⅰ作为经血宁颗粒的质量控制标准物质。From Mallotus apelta （ Lour.） Muell. -Arg one of JingXueNing granules component,compoundⅠwas getted by the separation and puri-fication and was identified it as flavoniods by qualitative identification. Compounds Ⅰis the single pure compounds by HPLC;the molecular weight of compound Ⅰis 564 by the analysis of MS. The data analysis of 1H NMR and 13C NMR from compoundⅠ is consistent with Corymboside. So the compo-und Ⅰwas as standard quality control substance of JingXueNing granules.

关 键 词：白背叶 化合物Ⅰ 伞房决明苷 标准物质 Mallotus apelta (Lour ) Muell -Arg CompoundⅠ 

分 类 号：TQ42[化学工程]