盐酸克伦特罗残留检测研究进展  

Research Progress on Residue Detection of Clenbuterol Hydrochloride

作　　者：孙来玉[1] 尹莉[1] 姚婷 杨金田[1] 邵朝纲[1] 钱坤[1] 

机构地区：[1]湖州师范学院生命科学学院,浙江湖州313000 [2]湖州市质量监督检验所,浙江湖州313000

出　　处：《湖州师范学院学报》2014年第4期27-32,共6页Journal of Huzhou University

基　　金：浙江省公益性应用研究计划"分析测试"项目(2012C37027)

摘　　要：介绍了盐酸克伦特罗残留检测的样品前处理技术、分析测试方法,并绘制了样品前处理技术路线图.其样品前处理技术主要有沉淀、离心、液-液萃取、固相萃取、基体分散固相萃取、中空纤维液相微萃取、分散液相微萃取、固相微萃取、免疫亲和色谱、分子印迹、超临界萃取等.分析测试方法主要有化学分析法、色谱法、毛细管电泳法、电化学分析法、免疫学分析法、生物传感器法等.相对于色谱-质谱联用等仪器分析技术的高速发展,盐酸克伦特罗残留检测样品前处理技术发展较为缓慢.因此,发展快速、高效、高选择性、环境友好、易于标准化且与分析测试方法衔接配套的样品前处理技术非常重要.This paper reviews the analytical methods and sample pre-treatment techniques of clenbuterol residue detection.The technical routes of sample pre-treatment are plotted.Sample pre-treatment techniques mainly include precipitation,centrifugation,liquid-liquid extraction,solid phase extraction,matrix solid-phase dispersion,hollow fiber liquid-phase micro-extraction,dispersive liquid-liquid micro-extraction,solid phase micro-extraction,immunoaffinity chromatography,molecular imprinted polymer,supercritical fluid extraction,etc.Analytical methods mainly include chemical analysis,chromatography,capillary electrophoresis,immunoassay,electrochemical analysis,biosensor,etc.Relative to the rapid development of chromatography-mass spectrometry hyphenated techniques and other instrumental analysis techniques,sample pre-treatment of clenbuterol hydrochloride residue detection development is relatively slow,and therefore,the development of fast,efficient,highly selective,environmentally friendly,easy and standardized sample pre-treatment technology is very important.

关 键 词：克伦特罗 样品前处理 残留检测 

分 类 号：O65[理学—分析化学]