蒜头果油中神经酸的含量测定  

Content determination of nervonic acid from Malania oleifera oil

作　　者：罗爱勤[1,2] 王小妹[2] 刘春芳[2] 葛发欢[2] 

机构地区：[1]广州中医药大学中药学院,广州510006 [2]广州白云山汉方现代药业有限公司 中药提取分离过程现代化国家工程研究中心,广州510240

出　　处：《中国当代医药》2014年第14期14-16,共3页China Modern Medicine

摘　　要：目的 建立蒜头果油中神经酸含量测定的方法.方法 采用气相色谱法,毛细管柱为ZB-Wax（30.00 m×0.25 mm×0.50 μm）,神经酸为对照品,程序升温,采用FID检测器.结果 神经酸在0.3045～6.0900 mg/ml范围内呈良好线性关系,平均回收率为101.5％,RSD为2.12％.结论 本法简便、快速、准确、重复性好,可用于测定蒜果油中神经酸的含量.Objective To establish a method for the content determination of nervonic acid from Malania oleifera oiL Methods Nervonic acid was determined by gas chromatography with aera-external standard method.A capillary column ZB-Wax（30.00 m×0.25 mm×O.50 μm）was used with nervonic acid as external standard,temperature programming and FID detector were used. Results Nervonic acid presented a good linear correlation within range from 0.3045 to 6.0900 mg/ml. The average recovery of nervonic acid was 101.5%,RSD was 2.12%. Conclusion This method is simple,reliable,has good repeatability and can be used for quality control of Malania oleifera oil.

关 键 词：气相色谱法 蒜头果油 神经酸 含量测定 

分 类 号：R285[医药卫生—中药学]