血三七胶囊质量标准初步研究  

Preliminary study on the quality standard for Xuesanqi capsules

作　　者：胡亚京[1] 吴小燕[1] 苏汉文[2] 向梅先[1] 

机构地区：[1]中南民族大学药学院,武汉430074 [2]武汉大学人民医院,武汉430060

出　　处：《华中师范大学学报（自然科学版）》2014年第3期375-378,共4页Journal of Central China Normal University：Natural Sciences

基　　金：国家自然科学基金项目(31200264);武汉市科技攻关项目(201260523189)

摘　　要：建立血三七胶囊质量控制标准.采用薄层色谱法进行定性鉴别,用高效液相色谱法（HPLC）对血三七胶囊中槲皮素进行含量测定.结果表明：薄层定性条件适合,斑点清晰,HPLC定量方法分离效果好,线性范围0.10～0.8 μg（r=1）,平均回收率100.03％,RSD=0.64％.本法简便、快洁、准确,可作为血三七胶囊质量控制方法.To establish a quality standard for Xuesanqi capsules.TLC was used to identity quercetin qualitative in xuesanqi capsules.The quanlitative analysis method of quercetin for Xuesanqi capsules was determined by HPLC.Conditions of qualitative identity by TLC were suitable.The results of quantitative analysis by HPLC were suitable.The range of linear was between 0.10 μg to 0.80 μg.（R =1）,the recovery of average was 100.03％,RSD=0.64％.So,a conclusion was gained：the methods is simple,sensitive and suitable for the quality control of Xuesanqi capsules.

关 键 词：血三七胶囊 质量标准 槲皮素 

分 类 号：R944[医药卫生—药剂学]