RP-HPLC法测定橘红痰咳液中柚皮苷含量  

DETERMINATION OF THE CONTENT OF NARINGIN IN JUHONG TANKE LIQUID BY RP-HPLC

作　　者：王统康 王振中 

机构地区：[1]江苏省连云港市药品检验所,连云港222006 [2]江苏省连云港康缘制药有限责任公司,连云港222001

出　　处：《中国药品标准》2001年第1期33-35,共3页Drug Standards of China

摘　　要：目的:建立反相高效液相色谱法测定主药化橘红中柚皮苷的含量。方法:采用 ALLTIMA-C_(18)5MICRON柱,以甲醇—1％冰醋酸(40:60)为流动相,280nm为检测波长。结果:测得线性范围2.0～10.0μg/ml(r=0.9997),平均回收率为99.06％,RSD=1.16％。结论:方法准确、可靠,可作为质量控制的方法。Objective: To establish a RP-HPLC method for determination of the content of Naringin in Hua Ju Hong. Method: Using ALLTIMA-C185 MICRON as column,methanol-1% acetic acid solution (40 : 60)as the mobile phase,Detection wavelength was 280nm. Results: The linesr cirrelation was observed is the range 2. 0-10.0μg/ml(r = 0. 9997). The average recovery was 99. 06% ,RSD=1. 16%. Concu-sion: The method is accurate,reliable,for the quality control.

关 键 词：橘红痰咳液 柚皮苷 RP-HPLC法 含量 

分 类 号：R286.4[医药卫生—中药学] R286.0[医药卫生—中医学]