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作 者:闫丽珍[1] 张永安[1] 李锡武[1] 李志辉[1] 王锋[1] 刘红伟[1] 熊柏青[1]
机构地区:[1]北京有色金属研究总院有色金属材料及制备加工国家重点实验室,北京100088
出 处:《Transactions of Nonferrous Metals Society of China》2014年第4期939-945,共7页中国有色金属学报(英文版)
基 金:Project (2012CB723903) supported by the National Basic Research Program of China
摘 要:The microstructural evolution of Al-0.66Mg-0.85Si alloy was investigated by optical microscopy (OM), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and differential scanning calorimetry (DSC). The as-cast microstructure is typical dendritical structure, consisting of α(Al), Al(FeMn)Si, Mg2Si, AlCuMgSi and Si phases. The electron diffraction analyses indicate that the Al(FeMn)Si phase is Al15(FeMn)3Si2 and the AlCuMgSi phase is Q(Al1.9CuMg4.1Si3.3). There are two kinds of Mg2Si phases in the as-cast microstructure. One is formed in the casting process, and the other is formed in the cooling process after casting process is finished. The phases have different crystal structures. After homogenization treatment at 545 ℃ for 20 h, Mg2Si, Si and Q intermetallic compounds are dissolved into matrix completely, and the remaining phases are α(Al) and Al15(FeMn)3Si2. The size of Al15(FeMn)3Si2 phase is decreased, and the phase is spheroidized and distributes along grain boundary discontinuously. The Zn-containing phases are not found during solidification and homogenization process.采用金相显微镜、扫描电子显微镜、透射电子显微镜和差示扫描量热法研究Al-0.66Mg-0.85Si合金在均匀化过程中的组织演变。合金铸态组织呈典型的枝晶形貌,存在α(Al)、Al15(FeMn)3Si2、Mg2Si,、Q(Al1.9CuMg4.1Si3.3)和Si相。铸态组织中存在2种不同晶体结构的Mg2Si相,一种是在铸造过程中形成的,另一种是在铸造完成后的空冷过程中形成的。经过545°C、20 h均匀化处理之后,组织中的Q、Mg2Si和Si相已完全溶入基体,残留的第二相主要是Al15(FeMn)3Si2相。Al15(FeMn)3Si2相的尺寸减小、球化并且在晶界上断续分布。在铸态和均匀化热处理状态中,均未发现含Zn相。
关 键 词:Al-Mg-Si alloy microstructural evolution HOMOGENIZATION intermetallic compound
分 类 号:TG146.21[一般工业技术—材料科学与工程]
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