补肾强身胶囊中淫羊藿苷的含量测定  

Determine the content of epimedium glycoside in the kidney and strength capsule

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作  者:龚玲 徐林[2] 孙月华[3] 

机构地区:[1]贵州省安顺市食品药品检验所,安顺561000 [2]贵州省安顺市疾病预防控制中心,安顺561000 [3]安顺学院,安顺561000

出  处:《北方药学》2014年第6期1-2,共2页Journal of North Pharmacy

摘  要:采用高效液相色谱法测定补肾强身胶囊中淫羊藿苷的含量。以XB-C18为色谱柱,以乙腈-水(30∶70)为流动相,以270nm为检测波长,流速为1.0ml/min,柱温为30℃。淫羊藿苷在16.576-165.76ug/ml的浓度范围内线性关系良好,R^2=1,平均回收率为100.2%,RSD%为0.74%。该方法简便、快捷、准确,能有效地控制补肾强身胶囊的质量。Using high performance liquid chromatography (HPLC)method was developed for the determination of epimedium glycoside in kidney and strengthen the capsule content. For XB - C18 chromatographic column, with acetonitrile - water (30∶70)as mobile phase, detection wavelength for 270nm, the flow rate of 1.0 ml/min, column temperature 30℃. Epimedium glycoside in 16.576 to 165.76ug/ml concentration range inside sex good, R^2=1, the average recovery was 100.2%, RSD % to 0.74%. The method is simple, quick, accurate, and can effectively control the quality of the kidney and strengthening the capsule.

关 键 词:高效液相色谱法 补肾强身胶囊 淫羊藿苷 

分 类 号:R927.2[医药卫生—药学]

 

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