气相色谱/质谱法测定水中五氯酚  

Determination of Pentachlorophenol in Water Using GC/MS

作　　者：范苓[1] 夏豪刚[1] 

机构地区：[1]苏州市环境监测中心站,江苏苏州215004

出　　处：《环境监测管理与技术》2001年第1期33-34,共2页The Administration and Technique of Environmental Monitoring

摘　　要：用GC/MS法测定环境水体和废水中的五氯酚 ,选择乙酸酐作衍生化试剂 ,二氯甲烷为萃取剂 ,比较了不同的衍生pH条件 ,以m/z为 2 6 6的定量特征离子定量 。To determine pentachlorophenol in water using GC/MS. Taking acetic anhydride as derivative reagent, methylene chloride as extracting agent, derivative pH conditions was compared, and the ion which m/z was 266 was selected for determination. The results were high sensitive and selective.

关 键 词：气相色谱 质谱法 五氯酚 水质测定 衍生化试剂 乙酸酐 萃取剂 二氯甲烷 

分 类 号：X832.02[环境科学与工程—环境工程]