双波长薄层扫描法测定腰腿痛丸中麻黄碱含量  被引量:1

Determination of Ephedrine Content in Yaotuitong Pill by TLC-densitometry

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作  者:尚立霞[1] 张玲[1] 胡庆文[1] 单卫华[1] 郭承军[1] 时延增[1] 

机构地区:[1]山东省生物药物研究院,山东济南250014

出  处:《时珍国医国药》2001年第5期400-401,共2页Lishizhen Medicine and Materia Medica Research

摘  要:目的 :采用双波长薄层扫描法测定腰腿痛丸中麻黄碱的含量。方法 :样品超声处理 ,离心后取上清液 ,在 λS=5 1 5 nm,λR=6 80 nm下测定含量。结果 :方法简便、准确度高 ,精密度好。结论Objective:This paper reported a method of quantitative analysis for ephedrine content in Yaotuitong Pill by TLC densitometry. Methods:The samples were extracted with ultrasonic treatment, were seperated by TLC after centrifugalization, then determined at λ S =515 nm, λ R =680 nm. Results:The result proved that the method was simple, rapid and accurate. Conclusion:It is suitable for the determination of ephedrine content in Yaotuitong Pill.

关 键 词:腰腿痛丸 薄层扫描法 麻黄 麻黄碱 中药 含量 

分 类 号:R284.1[医药卫生—中药学]

 

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