电合成对溴苯甲醛的气相色谱分析  

The GC Analysis of p-Bromobenzaldehyde in Electrosynthesis

作　　者：沈纬[1] 刘建稳[1] 王光信[1] 

机构地区：[1]青岛化工学院应用化学系,山东青岛266042

出　　处：《精细化工》2001年第3期181-182,185,共3页Fine Chemicals

摘　　要：建立了用气相色谱法同时测定电合成芳醛工艺中对溴苯甲醛和对溴甲苯的方法。选用OV - 17为固定相 ,正十四烷为内标物 ,在选定的色谱条件下分别用归一化法和内标法测定样品 ,结果 ,标准偏差≤ 0 3% ,回收率为 99 7%～ 10 1 0 % ,分析结果与常规的化学分析法吻合 ,该方法简便、快速、准确。The optimum conditions of GC Analysis were investigated for sample of p-bromobenzaldehyde in electrosynthesis. OV - 17 was chosen as stationary phase and n-tetradecane as internal standard. The results indicated that this method was rapid and accurate. The standard deviation was lower than 0.3% and the rate of recovery was 99.7% - 101.0%.

关 键 词：对溴苯甲醛 气相色谱法 电合成 归一化法 内标法 

分 类 号：TQ244.4[化学工程—有机化工]