高效液相色谱法分离测定硝胺火药中的NGu、RDX、NG、C_2和DBP  

Determination of Nitroguanidine (NGu) Nitroglycerine (NG) Centralite Ⅱ(C_2) and Dibuthyl Phthalate (DBP) in Nitramine Powder by High Performance Liquid Chromatography

作　　者：张国安[1] 胡新题 陈巨玉 陈洁 

机构地区：[1]华东工学院化工分院,南京210014

出　　处：《色谱》1991年第5期318-320,共3页Chinese Journal of Chromatography

摘　　要：硝胺火药是一种新型的科研发射药,具有高能耐高压的特点。硝胺火药组分中含有硝化纤维素(NC),硝化甘油(NG),2号中定剂(C_2)、苯二甲酸二丁酯(DBP),还含有高能炸药黑索金(RDX)和硝基胍(NGu),以提高火药的能量,但给分析测定却带来相当大的困难。A method for the rapid separation and detemination of NGu,RDX,NG,C2and DBP in RDU-5 Nitramine Powder has been developed by HPLC.The chromatographic conditions were:100×7.9mmi.d.radial compression column with micro Bondapak C18(10μm);1.5ml/ min methanol-water,80% (v/v) as eluant and UV-210nm detector.TNF and C1 were used as two internal standards.

关 键 词：硝胺火药 分析 高效液相色谱 

分 类 号：TQ562.2[化学工程—炸药化工]