三(4-氯苯甲酸)纤维素酯的合成及其作为色谱固定相的性能研究  

Synthesis of cellulose tris(4-chlorobenzoate) as gas chromatographicstationary phase and its characterization

作　　者：施介华[1] 杨根生[1] 郑云峰[1] 徐敏[1] 

机构地区：[1]浙江工业大学药学院,浙江杭州310032

出　　处：《浙江工业大学学报》2001年第4期383-385,共3页Journal of Zhejiang University of Technology

基　　金：浙江省分析测试基金资助项目 ( 0 0 0 35 )

摘　　要：采用催化合成法合成了三 (4 氯苯甲酸 )纤维素酯 ;并负载于GasChromQ载体上 ,用不同类型的探针分子表征其作为气相色谱固定相时的吸附性能 ,在其固定相上成功地分离了正构醇 (C1～C6)。The cellulose tris(4-chlorobenzoate) has been synthesised by the catalytic method and was supported on Gas Chrom Q. The adsorption capability of cellulose tris(4-chlorobenzoate) used as a gas chromatographic stationary phase was characterized by a variety of probe molecules. And, n-alcohols (C-1-C-6) were successfully separated on the cellullose tris(4-chlorobenzoate) stationary phase.

关 键 词：三(4-氯苯甲酸)纤维素酯 色谱固定相 吸附性能 催化合成 正构醇 

分 类 号：TQ352.71[化学工程] O657.7[理学—分析化学]