薄层扫描法测定元胡止痛滴丸中延胡索乙素的含量  

Determination of Tetrahydropalmatine in Yuanhuzhitong Dropping Pills by TLC-scanning

作　　者：杨玲霞[1] 王兰霞[1] 张伯崇[1] 

机构地区：[1]甘肃省药品检验所,甘肃兰州730000

出　　处：《中成药》2001年第12期869-871,共3页Chinese Traditional Patent Medicine

摘　　要：目的 :采用薄层扫描法对元胡止痛滴丸中延胡索乙素进行含量测定。方法 :样品经适当提取、净化后点于硅胶G薄层板上 ,以甲苯 无水乙醇 (2 0∶2 ,氨蒸气饱和 30min)为展开剂 ,置紫外灯 (2 5 4nm)下定位 ,检测波长为λS=2 80nm ,λR=310nm。结果 :平均回收率为 98.90 % ,RSD =3.10 %。结论 :此方法简单、准确 。Objective: To determine the content of tetrahydropalmatine in Yuanhuzhitong Dropping Pills by TLC scanning. Methods: The extraction solution of the sample was analyzed on silica gel G plate, with toluene anhydrous alcohol (20∶2, saturating for 30 min) as the developing system. The spot was located under UV (at 254nm), then detected by dual wavelength scanning (λ S=280nm,λ R=310nm). Results: The average recovery was 98.90%. RSD was 3.10%. Conclusion: The method is simple, accurate and available for the quality control of Yuanhuzhitong Dropping Pills.

关 键 词：元胡止痛滴丸 延胡索乙素 薄层扫描法 

分 类 号：R286.0[医药卫生—中药学]