复合型硅烷偶联剂的制备及表征  

Preparation and characterization of silane coupling complexes

作　　者：林海丹 董巍[2] 列剑平 杨明 崔明 刘赫 孙友群 梁永久 LIN Hai-dan;DONG Wei;LIE Jian-ping;YANG Ming;CUI Ming;LIU He;SUN You-qun;LIANG Yong-jiu(State Grid Jlhn Electric Power Co.,Ltd,Electric Power Research Institute,Changchun 130021,China;Changehun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun 130022,China)

机构地区：[1]国网吉林省电力有限公司电力科学研究院,吉林长春130021 [2]中国科学院长春应用化学研究所,吉林长春130022

出　　处：《分子科学学报》2018年第6期486-489,I0004,共5页Journal of Molecular Science

基　　金：国家自然科学基金资助项目(51673194);吉林省电力有限公司招标项目(SGTYHT/15-JS-194)

摘　　要：采用等物质的量的3-缩水甘油醚氧基丙基三甲氧基硅烷与三乙酰氧基乙烯基硅烷在120℃~150℃下反应3~5h,制备了复合型硅烷偶联剂,并通过红外光谱、核磁共振、气相色谱和质谱等方法对制备的偶联剂复合物进行了表征.The amount of substances such as γ-(2,3-epoxypropoxy)propyltrimethoxysilane and vinyltriacetoxysilane were reacted at 120℃~150℃ for 3~5 h,and then silane coupling agent complex was prepared.The properties of the silane coupling agent were determined by FTIR,NMR,GC and MS.

关 键 词：硅烷偶联剂 3-缩水甘油醚氧基丙基三甲氧基硅烷 三乙酰氧基乙烯基硅烷 

分 类 号：O622[理学—有机化学]