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作 者:金建南[1] 许盛昌[1] 张叔渊[1] 陈明生[1] 周懋伦[1]
机构地区:[1]四川大学原子核科学技术研究所
出 处:《同位素》1991年第1期15-19,9,共6页Journal of Isotopes
摘 要:本文介绍了在国产1.2m回旋加速器上通过^(109)Ag(d,2n)^(109)Cd核反应,从12.3MeV氘核辐照过的天然银靶中分离与制备无载体^(109)Cd的程序。银靶用HNO_3溶解后,利用金属铜经过电化学置换把银除去,再在混合的HNO_3/HBr介质中通过阴离子交换将^(109)Cd与Cu,^(65)Zn等其它元素定量分离。在制得的^(109)Cd产品中无其它放射性杂质存在(^(109)Cd>99.9%),^(109)Cd的回收率为99%。用陶瓷片吸附或电镀法制得了^(109)Cd的低能Υ和X射线源。A procedure is presented for the production and separation of carrier-free ^(109)Cd from irradiated natural silver target with 12.3 MeV deuterons via the ^(109)Ag(d, 2n) ^(109)Cd reaction at a domestic 1.2m cyclotron. After the target was dissolved with HNO_3, silver was removed by electrochemical displacement with copper metal, and ^(109)Cd was quantitatively separated from Cu, Zn and other elements by anion exchange in a mixed HNO_3/HBr medium. Almost no radioimpurities are present in ^(109)Cd obtained (^(109)Cd>99.9%) . The recovery is 99%. The low-energy γ and X-ray source of ^(109)Cd is prepared by adsorbing ^(109)Cd on a ceramic disk or electroplating method.
分 类 号:TL929[核科学技术—核燃料循环与材料]
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