石墨炉原子吸收法测定燃料油中金属钒  

DETERMINATION OF METALLIC VANADIUM CONTENT IN FUEL OIL BY GRAPHITIC FURNACE ATOMIC ABSORPTION SPECTROSCOPY

作　　者：陈信悦[1] 孙延伟[1] 于孝展[1] 杨春光[1] 

机构地区：[1]辽宁出入境检验检疫局技术检验中心,大连116001

出　　处：《精细石油化工》2002年第2期57-58,共2页Speciality Petrochemicals

摘　　要：将试样在坩埚内燃烧 ,灰化后 ,用盐酸溶解 ,用石墨炉原子吸收法测定钒含量。实验表明 ,该法回收率98%～ 1 0 2 % ,能满足日常检验钒含量在 0～ 1 0 0The samples were burnt in the crucible and ashed in the furnace at 600 ℃, dissolve the residue in HCL to make a solution for testing, then determine the vanadium in the fuel oil using graphitic furnace Atomic absorption spectroscopy. The testing results indicated that the recovery ratio is 98%102%. This method can satisfy the requirement of everyday tests while the vanadium content is in the range of 0100 μg/g.

关 键 词：石墨炉原子吸收法 测定 燃料油 金属钒 钒卟啉化合物 原子吸收法谱法 偏钒酸铵 

分 类 号：TE626.2[石油与天然气工程—油气加工工程] TE622.13