福建近海姥鲨肝油中角鲨烯的分离测定  被引量:12

Isolation and Determination of Squalene from the Liver of Cetorhinus maximus in Fujian Coastal

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作  者:王军[1] 翁幼竹[1] 苏永全[1] 郑微云[2] 余群[2] 

机构地区:[1]厦门大学海洋学系,福建厦门361005 [2]厦门大学环境科学研究中心,福建厦门361005

出  处:《厦门大学学报(自然科学版)》2002年第4期506-508,共3页Journal of Xiamen University:Natural Science

摘  要:采用薄层层析和气相层析法分离、检测了福建近海姥鲨 (Cetorhinusmaximus)幼鱼肝脏中角鲨烯含量 ,结果表明 :1)采用正已烷为展开剂的薄层层析法 ,碳氢化合物中角鲨烯的回收率可达 95 % ;2 )姥鲨肝脏中肝油和碳氢化合物含量存在明显的性别差异 ,但肝脏和肝油中角鲨烯含量无明显性别差异 ,分别为 0 .31% (♀ )、0 .32 % (♂ )和 0 .4 0 %(♀ )、0 .4 6 % (♂ ) ;3)Squalene from the livers of shark Cetorhinus maximus collected from Pingtan Island, Fujian Province was isolated and determined by thin layer chromatography and gas chromatography. The results showed: 1) the recovery rate of squalene isolated from hydrocarbon of the shark by thin layer chromatography with the eluent of n hexane was 95%; 2) there were obvious differences in contents of oil and hydrocarbon in livers between female and male shark, but contents of squalene in liver and oil of the shark liver seemed almost the same, with 0.31%(♀)?0.32%(♂) and 0.40%(♀)?0.46%(♂) respectively; 3) contents of sequalene of C. maximus were much richer than those of other sharks and rays collected from Fujian coastal.

关 键 词:角鲨烯 姥鲨 肝油 含量测定 薄层层析法 气相层析法 药用价值 福建近海 分离 

分 类 号:R284.2[医药卫生—中药学] Q959.423[医药卫生—中医学]

 

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