固溶时间对镍基单晶高温合金中Re,Ru元素分布和微观形貌的影响  

The effect of solution treatment time on the distribution of Re,Ru and the microstructure of nickel-based single crystal superalloys

作　　者：李宪[1] 张晓娜[1] 于潇翔 王崇愚[2,3] 于涛[3] 张泽[4] 

机构地区：[1]北京工业大学固体微结构与性能研究所,北京100124 [2]清华大学物理系,北京100084 [3]钢铁研究总院,北京100081 [4]浙江大学电镜中心,材料科学与工程学系,浙江杭州310027

出　　处：《电子显微学报》2014年第4期318-323,共6页Journal of Chinese Electron Microscopy Society

基　　金：国家自然科学基金重大仪器项目(No.11327901);国家重点基础研究发展规划项目(No.2011CB606402)

摘　　要：本文利用光学显微镜、扫描电子显微镜及X射线能谱仪,研究了固溶时间对镍基单晶高温合金中Re,Ru元素分布以及合金微观形貌的影响。结果表明,固溶时间为1 h时,Re,Ru均存在明显的枝晶偏析,固溶时间延长至20 h时,Re的枝晶偏析行为得到很大改善,Ru的分布基本趋于均匀。与Re相比,Ru的扩散速率相对较快。与固溶时间为1 h时的形貌相比,固溶20 h后合金中γ'相形貌更规则,立方度更好。The effect of solution treatment time on the distribution of Re,Ru and the microstructure of nickel-based single crystal superalloys were investigated by optical microscopy,scanning electron microscopy and energy dispersive spectrometer. The results show that the composition distribution of Re and Ru is in a state of apparent dendritic segregation with 1 hour＇s solution treatment time,while when the solution treatment time is extended to 20 hours,the dendritic segregation of Re is greatly improved,and the distribution of Ru is almost uniform. This indicates that the diffusion rate of Ru is faster than that of Re. Compared with the microstructure with 1hour＇s solution treatment time,the morphology of γ＇ phase is more regular with 20 hours＇ solution treatment time.

关 键 词：镍基单晶高温合金 固溶处理 元素分布 微观形貌 

分 类 号：TG132.3[一般工业技术—材料科学与工程] TG156.94[金属学及工艺—合金]