爱维心口服液质量标准研究  

A Study on Quality Standard of Aiweixin Oral Liquid

作　　者：穴卓 李玥瑛 张清波 张树杰 

机构地区：[1]黑龙江中医药大学,黑龙江哈尔滨150040 [2]黑龙江省食品药品检验检测所,黑龙江哈尔滨150001 [3]黑龙江省食品药品监督管理局,黑龙江哈尔滨150020

出　　处：《中国中医药信息杂志》2014年第11期82-84,共3页Chinese Journal of Information on Traditional Chinese Medicine

摘　　要：目的：建立爱维心口服液质量标准。方法采用薄层色谱法对制剂中的丁香、西红花进行鉴别,采用气相色谱法测定丁香中丁香酚的含量。结果丁香、西红花的薄层色谱特征斑点分离清晰,阴性对照无干扰。丁香酚在0.05217～2.0868μg范围内线性关系良好（r＝0.9999）,供试品溶液在24 h内稳定,平均加样回收率为95.7%,RSD＝1.4%（n＝6）。结论本方法简单、准确可靠、重复性好,可用于控制爱维心口服液的质量。Objective To establish a quality standard for Aiweixin oral liquid. Methods TLC was applied to the identification of Caryophylli Flos and Crocin in Aiweixin oral liquid. Eugenol was analyzed by GC. Results TLC of Caryophylli Flos and Crocin had distinct separation of characteristic spots and there was no interference in negative comparison. The linear response ranges of Eugenol were between 0.052 17-2.086 8μg （r=0.999 9）. The samples were steady within 24 h. The average recovery of eugenol was 95.7%, RSD=1.4% （n=6）. Conclusion The method is simple, accurate and reliable, and can be used for the quality control of Aiweixin oral liquid.

关 键 词：爱维心口服液 丁香 西红花 丁香酚 薄层色谱法 气相色谱法 

分 类 号：R284.1[医药卫生—中药学]