两种不同提取方法所得莪术油的成分对比分析  

Comparison of Components in Essential Oils of Curcuma wenyujin Y. H. Chen et C. Ling Obtained by Two Different Methods

作　　者：刘布鸣[1] 苏小川[2] 白懋嘉 林霄[1] 柴玲[1] 

机构地区：[1]广西中医药研究院/广西中药质量标准研究重点实验室,广西南宁530022 [2]广西疾病预防控制中心,广西南宁530022 [3]南宁万家辉香料有限公司,广西南宁530022

出　　处：《香料香精化妆品》2014年第5期1-7,共7页Flavour Fragrance Cosmetics

基　　金：广西自然科学基金资助项目(桂科基0832024);广西中药质量标准研究重点实验室系统性研究项目(桂中重系201306)

摘　　要：利用气相色谱、气相色谱-质谱联用分析技术,对水蒸气蒸馏和超临界CO2萃取两种不同方法提取得到的莪术油化学成分进行分析鉴定,分别从中分离出60余和90余个组分,并确认了其中50多种化学成分,得到鉴定的组分峰面积占总馏出峰面积的90%以上。根据成分鉴定结果,对不同提取方法所得莪术油的主要化学成分进行比较分析。两种不同提取方法获得的莪术油组分不完全相同,含量也不尽相同,但主要化学成分基本一致,超临界CO2萃取的莪术油所含化学成分较多且相对分子质量较大的重组分较多。同时,对不同方法提取的莪术油中莪术醇等主要特征成分,采用薄层色谱、气相色谱、质谱进行分析测定。研究结果可为莪术油的开发与质量控制提供科学依据。Two kinds of essential oil were obtainted from Curcuma wenyujin Y. H. Chen et C. Ling by steam distillation and SFE-CO2 respectively. TLC,GC and GC-MS method were applied to analyze and compare the components in them. Over 60 and 90 components were separated from these two kinds of oil respectively,and over 50 components were confirmed among them. The results showed that the components in these two oils and their relative contents were not exactly the same,but the main constituents were similar. There were more heavy components in the essential oil obtained by SFE-CO2. The results provided a scientific basis for the development and quality control of essential oil of Curcuma wenyujin Y. H. Chen et C. Ling.

关 键 词：莪术油 气相色谱 气相色谱-质谱联用分析 化学成分 比较分析 

分 类 号：R284[医药卫生—中药学]