顶空气相色谱法检测卫生用纸中的氧乙烯基含量  

Determination of Oxyethylene Groups in Tissue Paper by Headspace Gas Chromatography

作　　者：余伟梅 田迎新[2] 胡会超[3] 柴欣生[1,2] 陈春霞 陈润权 

机构地区：[1]国家纸制品质量监督检验中心,广东东莞5230808 [2]华南理工大学制浆造纸工程国家重点实验室,广东广州510641 [3]福建农林大学材料工程学院,福建福州350002

出　　处：《造纸科学与技术》2014年第5期64-67,87,共5页Paper Science & Technology

基　　金：国家质检总局质检公益性行业科研专项经费资助项目(2012104018-1)

摘　　要：本文建立了一种基于顶空气相色谱技术的卫生纸和纸巾纸中氧乙烯基含量的检测方法,该方法通过萃取、浓缩、高温反应等过程,将样品中的氧乙烯基转化为能够用顶空气相色谱检测的碘乙烷,与传统方法相比本文方法简便、安全、灵敏度高。This paper reports a headspace gas chromatographic technique for determination of oxyethylene groups in tissue paper. The oxyethylene groups of polymers in tissue paper were converted to iodoethane in hydroiodic acid medium in a closed vial after sample extraction and concentration. The iodoethane was then detected by headspace gas chromatography. The present method is simple, safety and high sensitivity compared with the traditional method.

关 键 词：顶空气相色谱 卫生纸和纸巾纸 氧乙烯基 碘乙烷 

分 类 号：TS77[轻工技术与工程—制浆造纸工程]