参芪益气固本片质量标准研究  

Shen Qi Yi Qi Gu Ben Tablet quality standard

作　　者：王世华[1] 刘少琴[1] 陈浩源[1] 李坤[1] 王永[1] 

机构地区：[1]河北石家庄以岭药业股份有限公司,河北石家庄050035

出　　处：《中医学报》2014年第B12期70-72,共3页Acta Chinese Medicine

摘　　要：目的制定参芪益气固本片的质量控制方法.方法：采用薄层色谱法对人参、白芍、当归、连翘、制首乌进行薄层鉴别,采用高效液相色谱法测定了制剂中芍药苷的含量.结果：通过方法学考察,表明芍药苷进样量在65.5-2068.2 ng 内有良好的线性关系.芍药苷的平均回收率为98.24%（n=9）,RSD 为1.58%.结论：方法快捷、准确、重现性好、精密度高,适用于参芪益气固本片的质量控制.Objective To establish the quality control method of Shen Qi Yi Qi Gu Ben Tablet Methods： TLC ginseng, white peony root, angelica, forsythia, Radix carriedTLC measured Paeoniflorin content preparation by HPLC. Results： The methodological study showed that the injection volume Paeoniflorin a good linear relationship within 65.5 -3068.2 ng. The average recovery of paeoniflorin was 98.24% （n = 9）, RSD was 1.58%. Conclusion： The method is fast, accurate, reproducible, high precision, Shen Qi Yi Qi Gu BenTablet suitable for quality control of the film.

关 键 词：薄层鉴别 高效液相色谱法 芍药苷 人参 

分 类 号：R563[医药卫生—呼吸系统]