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机构地区:[1]武汉市第一医院药学部,武汉430022 [2]浙江科技学院生物与化学工程学院 [3]四川大学化学工程学院
出 处:《中国药师》2015年第1期66-68,共3页China Pharmacist
摘 要:目的:优化乌饭树树叶中总黄酮的超声提取工艺。方法:采用单因素试验和正交设计,以总黄酮的含量为指标,以提取溶剂浓度、料液比、提取时间、提取次数为试验因素,优化乌饭树树叶中总黄酮的超声提取工艺。结果:优化试验方案所得乌饭树树叶中总黄酮最佳提取工艺为:70%乙醇,料液比为1∶40,提取时间30 min,提取次数2次。结论:该提取工艺稳定、可行,研究结果可为改进现有乌饭树树叶总黄酮的提取工艺提供有益参考。Objective:To optimize the ultrasound-assisted extraction process of total flavonoids in Vaccinium bracteatum Thunb. leaves. Methods:The single factor test and orthogonal test were adopted with the content of total flavonoids as the index, and the ultra-sound-assisted extraction was optimized with the concentration of solvent, extracting time, ratio of raw material to liquid and extraction times as the factors. Results:The optimal extraction conditions were 70% ethanol with 40-fold volume, extracting 2 times with 30 mi-nutes per time. Conclusion:The extraction process is stable and feasible, and all the results are useful references for the extraction process improvement.
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