醋京大戟饮片质量标准研究  

Quality standard for pieces of Euphorbia pekinensis processed with vinegar

作　　者：葛秀允[1] 张乐林[1] 孙立立[1] 

机构地区：[1]山东省中医药研究院,国家中医药管理局中药蜜制和制炭炮制技术与原理研究重点实验室,山东济南250014

出　　处：《时珍国医国药》2015年第3期628-630,共3页Lishizhen Medicine and Materia Medica Research

基　　金：国家中医药管理局中医药行业科研专项(No.200807039)

摘　　要：目的对不同批次醋京大戟饮片样品进行分析,建立醋京大戟饮片的质量标准。方法以大戟二烯醇为对照品,采用薄层层析法和高效液相色谱法对醋京大戟饮片进行了定性和定量研究;并对醋京大戟饮片进行杂质检查,对灰分、水分和浸出物含量进行了测定。结果不同批次的醋京大戟饮片在杂质、水分和浸出物含量等方面均存在差异。薄层鉴别色谱斑点清晰,分离度较好。所建立的含量测定方法操作简单、准确、重现性好。结论建立了较为完善的醋京大戟饮片质量标准,填补了醋京大戟饮片质量标准方面的空白。Objective To establish quality standard of Euphorbia pekinensis processed with vinegar by studying different batches pieces of Euphorbia pekinensis processed with vinegar. Methods Taking euphol as reference substances,qualitative identification and quantitative detection of pieces Euphorbia pekinensis processed with vinegar was stuidied by TLC and HPLC,and impurities,moisture,ash and extract contents of pieces of Euphorbia pekinensis processed with vinegar in different batches was researched. Results the nomal and science quality standard of Euphorbia pekinensis processed with vinegar was established. Conclusion the quality standard filling a domestic gap in pieces of Euphorbia pekinensis processed with vinegar.

关 键 词：醋京大戟 大戟二烯醇 质量标准 

分 类 号：R284.1[医药卫生—中药学] R283[医药卫生—中医学]