丙烯酸-2-乙基己酯气相色谱填充柱的制备及其应用  

Preparation and Application of Packed Column 2-Ethylhexyl Acrylate Gas Chromatography

作　　者：刘志[1] 范翠萍[1] 

机构地区：[1]中海油能源发展股份有限公司惠州石化分公司化验中心,广东惠州516086

出　　处：《广东化工》2015年第5期30-31,共2页Guangdong Chemical Industry

摘　　要：根据丙烯酸-2-乙基己酯纯度检测的要求,自制色谱柱并用于丙烯酸-2-乙基己酯纯度的分析,考察了固定相的组成和涂渍对检测的影响,建立定量分析方法,实验结果表明在选定的色谱条件下,能够准确分析其中杂质,仪器稳定性较好,检测重现性较好,RSD符合国家标准[1]对检测的要求。According to the 2-Ethylhexyl acrylate purity testing requirements,home-made chromatographic column and used to analyze 2-Ethylhexyl acrylate purity,effects of stationary phase composition and coating on the detection,the establishment of quantitative analysis method,the experimental results show that the selected chromatographic conditions,can accurate analysis of impurities,instrument stability is better good reproducibility,detection,RSD meet the national standards on detection.

关 键 词：丙烯酸-2-乙基己酯 填充柱 涂渍 制备 

分 类 号：TQ[化学工程]