N,N-二烯丙基-5-甲氧基色胺片剂的GC/MS检验  

Identification of N,N-diallyl-5-methoxytryptamine in Seized Tablets by GC/MS

作　　者：郑水庆 梁晨 王威 张润生 

机构地区：[1]上海市毒品检验中心上海市现场物证重点实验室,上海200083

出　　处：《刑事技术》2015年第2期166-167,共2页Forensic Science and Technology

摘　　要：目的建立N,N-二烯丙基-5-甲氧基色胺的气相色谱-质谱(GC/MS)定性分析方法。方法未知片剂样品用甲醇超声溶解,吸取上清液采用气相色谱-质谱(GC/MS)联用仪检测。结果测得未知组分(t R=10.45min)的质谱特征碎片峰(m/z)信息为110.1(基峰)、270.1、174.1、160.1、145.0、130.1和117.1。查阅资料并对该组分的质谱图谱进行解析,鉴定为N,N-二烯丙基-5-甲氧基色胺,属于色胺类化合物。结论该方法简单,准确,可用于N,N-二烯丙基-5-甲氧基色胺的鉴定。Objective To establish a method for identification of N,N-diallyl-5-methoxytryptamine by GC/MS. Methods The sample was extracted with methanol in ultrasonic bath. And the supernatant was injected into GC/MS. Results Unknown component（tR=10.45min） presented characteristic fragment ion peaks at m/z 110.1（base peak）, 270.1, 174.1, 160.1, 145.0, 130.1 and 117.1. According to relevant literatures and mass spectrometry analysis, this drug was identified as N,N-diallyl-5-methoxytryptamine. This compound belonged to tryptamines. Conclusions Method established in this paper is simple, accurate, and suitable for identification of N,N-diallyl-5-methoxytryptamine.

关 键 词：N N-二烯丙基-5-甲氧基色胺 GC/MS 色胺类化合物 定性分析 

分 类 号：D919.1[医药卫生—法医学]