何首乌中蒽醌类物质的超声波提取工艺优化  

Process optimization of ultrasonic extraction of the total anthraquinone from polygonum multiflorum

作　　者：黄小梅[1,2] 邓祥[1,2] 吴狄[1,2] 

机构地区：[1]四川文理学院化学化工学院,四川达州635000 [2]特色植物开发研究四川省高校重点实验室,四川达州635000

出　　处：《化学研究》2015年第2期166-169,共4页Chemical Research

基　　金：四川省教育厅重点项目资助(13ZA0101);"特色植物开发研究"四川省高校重点实验室项目资助(sctz201301;sctz201305)

摘　　要：采用超声波辅助法提取何首乌中蒽醌类物质.讨论了甲醇体积分数、提取时间、提取温度、料液比和提取功率5个因素对提取效率的影响;通过正交试验确定了何首乌中蒽醌类物质的最佳提取工艺条件,甲醇体积分数为80%,提取时间为1.0h,提取温度为45℃,料液比为1∶15(g∶mL),提取功率为700W.此条件下蒽醌类物质的最大提取率为1.472 9%.The total anthraquinones were extracted from polygonum multiflorum by ultrasonic method .The effects of five factors on the extraction ,including methanol concentration ,extrac‐ting times ,extracting temperature ,material/solvent ratio and extracting power were studied by single factor test .The optimal conditions of extraction were determined as follows ：metha‐nol volume fraction was 80% ,extracting time was 1 0. h ,extracting temperature was 45 ℃ , material‐solvent ratio was 1∶15 （g∶mL） and extracting power was 700 W .Under these oper‐ation conditions ,the maximum rate of extraction of the total anthraquinones was 1 4.72 9% .

关 键 词：何首乌 蒽醌 超声波 正交实验 

分 类 号：TQ914.1[化学工程]