16%辛硫磷·多菌灵悬浮种衣剂高效液相色谱分析  

HPLC analysis of 16% Phoxim-Carbendazim SE for Seed Coating

作　　者：王立石[1] 黄均伟[1] 刘洪丽[1] 陈有嗣[1] 李江岩[1] 

机构地区：[1]辽宁省蚕业科学研究所,辽宁凤城118100

出　　处：《辽宁农业科学》2015年第3期73-75,共3页Liaoning Agricultural Sciences

摘　　要：建立了一种高效液相色谱法同时测定16%辛硫磷·多菌灵悬浮种衣剂有效成分含量的分析方法。用Novapak C8不锈钢色谱柱,甲醇∶水∶四氢呋喃=60∶40∶20(V/V)为流动相,在254 nm波长下对16%辛硫磷·多菌灵悬浮种衣剂进行定量分析。辛硫磷和多菌灵的线性相关系数分别为0.997和0.998,标准偏差分别为0.034和0.058,变异系数分别为0.422%和0.719%,平均回收率分别为99.2%和99.4%。该方法操作简便,快速,准确,是辛硫磷·多菌灵悬浮种衣剂中有效成分的理想检测方法。The analysis method to establish HPLC method for the inspection of effective components of 16%phoxim-carbendazim SE for seed coating.Novapak C8 stainless steel column,methanol∶water∶tetrahydrofu-ran =60∶40∶20 （V /V）as the mobile phase,at 254 nm wavelength of 16% phoxim-carbendazim SE for seed coating quantitative analysis.Phoxim and carbendazim linear correlation coefficients were 0.997 and 0.998,the standard deviation were 0.034 and 0.058,the coefficients of variation were 0.422% and 0.719%,the average recoveries were 99.19% and 99.42% respectively.This method is simple,good lineari-ty,accuracy,precision,detection and analysis method is 16% phoxim-carbendazim suspension seed ideal.

关 键 词：辛硫磷 多菌灵 悬浮种衣剂 高效液相色谱 

分 类 号：O652[理学—分析化学]