一硫化四甲基秋兰姆的制备及其检测分析  

Preparation of Tetramethyl Thiuram Monosulfide with Its Test and Analysis

作　　者：李延升[1,2] 王振香 李红良 贾太轩[2] 张楠[2] 

机构地区：[1]鹤壁联昊化工股份有限公司,河南鹤壁458000 [2]安阳工学院化学与环境工程学院,河南安阳455000

出　　处：《广东化工》2015年第16期107-108,共2页Guangdong Chemical Industry

基　　金：国家自然科学基金资助课题(20776031)

摘　　要：本研究首先合成出了一硫化四甲基秋兰姆(TMTM),通过UV-vis、HPLC、XRD粉末衍射仪对其进行检测和表征,确定了TMTM的最大吸收波长,选择出合适的液相色谱条件,为企业建立产品工作标准品,评判TMTM的产品性能指标,为制定行业标准提供了实验依据。通过XRD粉末衍射仪测定TMTM的结构,得到的TMTM晶体学数据,为关联其性能和推断结构,提供基础实验数据。In the study, rubber accelerator tetramethyl thiuram monosulfide（TMTM） was synthesized firstly. TMTM was dete basic experiment data of TMTM crystallography data, associated with its performance and structure, provides the basic exp cted and characterized by UV-vis、HPLC、XRD. The maximum absorption wavelength of TMTM was determined. The suitable liquid chromatographic conditions were chosen. This study can help the enterprises to designate the working standard tracing detection of TMTM industrialized production. Performance index of TMTM was judged. It can provide the eriment data.

关 键 词：一硫化四甲基秋兰姆 工作标准品 UV-VIS HPLC XRD 

分 类 号：O657.3[理学—分析化学]