2,2’-硫代双对特辛基苯酚的合成改进  

The Improved Synthesis of 2,2'-thiobis(p-t-octylphenol)Sulfide

作　　者：高俊峰 李迁 刘东峰 

机构地区：[1]保定市乐凯化学有限公司,保定071000

出　　处：《信息记录材料》2015年第4期28-31,共4页Information Recording Materials

摘　　要：使用无水氯化锌做催化剂,以对特辛基苯酚与二氯化硫为主要原料,通过对二氯化硫的量,催化剂的量,滴加温度,溶剂等条件的优化,确定了合成2,2’-硫代双对特辛基苯酚的合理配料比,提高了收率。The functional molecule （AEHB） was prepared from acrylate acid via epoxidation and esterification. The hyperbranched oligomer was prepared from TMPTA via thermal initiation and terminated by AEHB. The photosensitive resin containing the photoinitiator was then used for 3D printing and a 3D object was obtained which had the efficiency up to 84% for removal of the formaldehyde.

关 键 词：2 2’-硫代双对特辛基苯酚 无水氯化锌 合成 

分 类 号：TQ2[化学工程—有机化工]