3-芳基苯并呋喃酮类化合物的精制工艺研究  

Research of purification technology and application of 3-Arylbenzofunanone analogues

作　　者：董平[1] 邵伟[1] 李建忠[1] 赵仲阳 何玉莲[1] 

机构地区：[1]大庆化工研究中心,黑龙江大庆163714

出　　处：《炼油与化工》2015年第5期17-20,共4页Refining And Chemical Industry

摘　　要：对3-芳基苯并呋喃酮衍生物3-(3,4-二甲基苯基)-5,7-二叔丁基-3-氢-苯并呋喃-2-酮(SHY-1)的精制工艺进行了研究。在较佳的精制工艺条件下,精制产品的纯度可达99.90%,收率可达70.20%;其在BOPP的应用效果显示,三元复合抗氧剂组成配比SHY-1为15%、1010为42.5%、并且168为42.5%的YJK-101-1#抗氧化效果最为突出。The purification process and application of 3-（3,4- dimethylphenyl）- 5,7- di- tert- butyl- methyl- 3H-benzofuran-2-one（SHY-1）was researched. The purification process conditions were optimized,the purity of the productwas 99.90% and the yield of the product was 70.20% under optimum purification condition. Its application effect on BOPPshowed that when the ternary composite antioxidant ratio is 15% for YJK-101-1#,42.5% for SHY-1,42.5% for 1010 and42.5% for 168,its anti-oxidation effect is most prominent.

关 键 词：3-芳基苯并呋喃酮 萃取结晶 精制 抗氧剂 

分 类 号：TQ21[化学工程—有机化工]