HS-SPME-GC/MS法分析石刁柏果皮及种子中挥发性成分  

Analysis of volatile constituents from peel and seeds ofAsparagus officinalis by HS-SPME-GC/MS

作　　者：魏金凤[1,2] 许艳东[1] 曹鹏然 刘宇[1] 乔笑笑 罗予婉 康文艺[1] 

机构地区：[1]河南大学中药研究所,河南开封475004 [2]河南大学民生学院,河南开封475004

出　　处：《河南大学学报（医学版）》2015年第4期244-246,共3页Journal of Henan University:Medical Science

基　　金：河南大学大学生创新创业训练计划项目(15NB075);河南省科技厅基础前沿计划(132300410255);河南省科技厅基础前沿计划(142300410123);河南省高等学校青年骨干教师资助计划项目(教高[2012]704号)

摘　　要：目的分析石刁柏果皮与种子的挥发性成分。方法采用顶空固相微萃取和气质联用技术(HS-SPMEGC/MS),结合保留指数法并用峰面积归一化法测定相对百分含量。结果从石刁柏果皮挥发油中鉴定出1个挥发性成分,占总峰面积的74.47%。石刁柏种子挥发油中鉴定出2个挥发性成分,占总峰面积的29.42%。结论石刁柏果皮的主要挥发性成分是十二酸乙酯(74.47%),种子的主要挥发性成分为十二酸乙酯(11.49%)和十六酸乙酯(17.93%)。Objective To assay the volatile constituents ofA.officinalis.Methods The volatiles were analyzed by head-space solid micro-extraction,coupled with GC/MS and Kovats.Results There is 1 kind of volatile constituents in peel of A.officinalis,and2 different kinds of volatile constituents in seeds.The content of the identified compounds extracted from peel and seeds were 74.47% and 29.42%.Conclusion The major volatile constituents of seedswere ethyl dodecanoate（11.49%）and ethyl hexadecanoate（17.93%）.The volatile constituent of peel was ethyl dodecanoate（74.47%）.

关 键 词：石刁柏 挥发性成分 固相微萃取 气质联用 

分 类 号：TQ460.7[化学工程—制药化工]