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作 者:石国梁[1] 张奎[1] 李兴刚[1] 李永军[1] 马鸣龙[1] 袁家伟[1] 卢春芳[1]
机构地区:[1]北京有色金属研究总院有色金属材料制备加工国家重点实验室,北京100088
出 处:《Transactions of Nonferrous Metals Society of China》2015年第12期3944-3952,共9页中国有色金属学报(英文版)
基 金:Project(2013CB632202)supported by the National Basic Research Program of China
摘 要:The mixed grain structure and mechanical property anisotropy of AZ40 magnesium alloy bar with a diameter of 160 mm manufactured by "multi-direction forging(MDF) + extrusion + online cooling" technique were investigated by optical microscopy(OM), scanning electron microscopy(SEM), X-ray diffraction macro-texture measurement and room temperature(RT) tensile test. The results show that mixed grain structure is caused by the micro-segregation of Al in semi-continuous casting ingot. Homogenization of(380 °C, 8 h) +(410 °C, 12 h) cannot totally eliminate such micro-segregation. During MDF and extrusion, the dendrite interiors with 3%-4% Al(mass fraction) transform to fine grain zones, yet the dendrite edges with about 6% Al transform to coarse grain zones. XRD macro-textures of the outer, R/2 and center show typical fiber texture characteristics and the intensity of [0001]//Ra D orientation in the outer(11.245) is about twice as big as those in the R/2(6.026) and center(6.979). The as-extruded AZ40 magnesium alloy bar has high elongation(A) and moderate ultimate tensile strength(Rm) in both extrusion direction(ED) and radius direction(Ra D), i.e., A of 19%-25% and Rm of 256-264 MPa; however, yield strength(Rp0.2) shows anisotropy and heterogeneity, i.e., 103 MPa in Ra D, 137 MPa in ED-C(the center) and 161 MPa in ED-O(the outer), which are mainly caused by the texture.(155 °C, 7 h) +(170 °C, 24 h) aging has no influence on strength and elongation of AZ40 magnesium bar.采用"多向锻造(MDF)+挤压+在线冷却"技术制备的AZ40(直径为160 mm)镁合金棒材具有混晶组织和力学性能各向异性,通过光学显微镜(OM)、扫描电镜(SEM)、X射线衍射织构测量和室温拉伸试验对上述特征进行表征和分析。结果表明:混晶组织来源于半连续铸锭中Al的微观偏析。均匀化处理((380°C,8 h)+(410°C,12 h))不能完全消除这种微观偏析。在后续MDF和挤压过程中,Al含量为3%-4%(质量分数)的枝晶心部转变成细晶区,而Al含量约为6%的枝晶边缘转变成粗晶区。表层、R/2和心部的XRD宏观织构都呈现典型的纤维织构特征,且表层的[0001]//Ra D取向强度(11.245)约为R/2处(6.026)和心部(6.979)的两倍。挤压态AZ40镁合金棒材沿挤压方向和半径方向具有优异的伸长率(A)和中等抗拉强度(Rm):A为19%-25%,Rm为256-264 MPa;然而,屈服强度(Rp0.2)呈现出各向异性和内外不均匀性,即Ra D为103 MPa,ED-C(心部)为137 MPa,ED-O(边部)为161 MPa,这主要是织构造成的。(155°C,7 h)+(170°C,24 h)时效处理对AZ40镁合金棒材的强度和伸长率几乎没有影响。
关 键 词:AZ40 magnesium alloy mixed grain structure mechanical properties ANISOTROPY MICRO-SEGREGATION texture
分 类 号:TG146.22[一般工业技术—材料科学与工程]
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