气相色谱法测定新雪片中冰片含量  

Determination Content of Borneol in Xinxue Tablets by GC

作　　者：肖琦 黄小兰 阳文武 朱泽兵 

机构地区：[1]万州食品药品检验所,重庆404000

出　　处：《亚太传统医药》2016年第5期39-40,共2页Asia-Pacific Traditional Medicine

摘　　要：目的:提高新雪片的质量标准。方法:安捷伦DB-WAX毛细管柱(30m×0.32mm,0.25μm),载气流速1.0mL/min,进样口温度180℃,柱温140℃,氢火焰离子化检测器(FID),检测器温度250℃。结果:该方法的精密度和准确度均好。结论:该方法结果准确,重复性好,可用于控制新雪片质量。Objective：To improve the standard of quality control of Xinxue Tablets. Methods：The Agilent DB-WAX column（30m × 0. 32mm, 0. 25μm） was used with nitrogen at a flow rate of 1.0mL/min, the injection port temperature was180℃, the column temperature was140℃ ,the FID detector temperature was 250℃. Results： The precious and accuracy were good. Conclusion：The method is accurate and better repeatable,which can be used for the quality control of XinXue Tablets.

关 键 词：新雪片 冰片 气相色谱法 含量测定 

分 类 号：R284.2[医药卫生—中药学]