气相色谱法测定邻氨基苯乙醚及其有机杂质  

Determination of o-Phenetidine and Organic Impurities by GC

作　　者：季浩[1] 黄银波 沈日炯[1] 

机构地区：[1]沈阳化工研究院有限公司,沈阳110021 [2]泰州市产品质量监督检验所,泰州225300

出　　处：《染料与染色》2016年第1期48-51,共4页Dyestuffs and Coloration

摘　　要：采用气相色谱对邻氨基苯乙醚及其有机杂质进行分离,用峰面积归一化法进行定量分析。通过气相色谱-质谱联用仪对邻氨基苯乙醚及其有机杂质进行分离并定性。使用精密度数据对分析方法进行了评价,给出了各杂质的最小定量限。o-Phenetidine and its organic impurities were separated by gas chromatography, and their contents were quantified by peak area normalization method, o-Phenetidine and its organic impurities were separated and qualified by GC-MS. The analysis method was e- valuated by the data of precision, and quantification limit of each impurity were provided.

关 键 词：邻氨基苯乙醚 气相色谱 峰面积归一化法 

分 类 号：TQ243.24[化学工程—有机化工] O657.71[理学—分析化学]