补肾益心片薄层鉴别研究  被引量:1

Study on TLC Differentiation for Bushen Yixin Tablet

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作  者:何嘉仑[1] 吴晓贞[1] 黄樱华[1] 

机构地区:[1]广州中医药大学第一附属医院,广东广州510405

出  处:《亚太传统医药》2016年第9期17-19,共3页Asia-Pacific Traditional Medicine

摘  要:目的:建立补肾益心片的薄层鉴别方法。方法:优化展开剂、点样量等色谱条件,建立了淫羊藿的薄层鉴别方法,并对其进行方法学验证。结果:最佳方法为:以乙酸乙酯-丁酮-甲酸-水(10∶1∶1∶1)为展开剂,点样量为供试品溶液及对照品溶液各4μL,该方法耐用性良好。结论:本法操作简便、快速,结果可靠,重复性好,可作为补肾益心片的质量控制方法。Objective:To establish the TLC method for Bushen Yixin Tablet.Methods:According to the optimization of developing solvent,sample quantity and the investigation of TLC plate,temperature,relative humidity,the TLC method of Bushen Yixin Tablet was established.Results:The optimal developing solvent was ethyl acetate-butanone-methanoic acid-water(10∶1∶1∶1);The optimal sample quantities of the sample solution and the control solution were 4microlitres;TLC plate,temperature and relative humidity had no influence on the results.Conclusion:The method is convenient,reliable and accurate for the quality control of Bushen Yixin Tablet.

关 键 词:补肾益心片 薄层鉴别 淫羊藿苷 

分 类 号:R286[医药卫生—中药学]

 

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