检索规则说明:AND代表“并且”;OR代表“或者”;NOT代表“不包含”;(注意必须大写,运算符两边需空一格)
检 索 范 例 :范例一: (K=图书馆学 OR K=情报学) AND A=范并思 范例二:J=计算机应用与软件 AND (U=C++ OR U=Basic) NOT M=Visual
机构地区:[1]广州中医药大学第一附属医院,广东广州510405
出 处:《亚太传统医药》2016年第9期17-19,共3页Asia-Pacific Traditional Medicine
摘 要:目的:建立补肾益心片的薄层鉴别方法。方法:优化展开剂、点样量等色谱条件,建立了淫羊藿的薄层鉴别方法,并对其进行方法学验证。结果:最佳方法为:以乙酸乙酯-丁酮-甲酸-水(10∶1∶1∶1)为展开剂,点样量为供试品溶液及对照品溶液各4μL,该方法耐用性良好。结论:本法操作简便、快速,结果可靠,重复性好,可作为补肾益心片的质量控制方法。Objective:To establish the TLC method for Bushen Yixin Tablet.Methods:According to the optimization of developing solvent,sample quantity and the investigation of TLC plate,temperature,relative humidity,the TLC method of Bushen Yixin Tablet was established.Results:The optimal developing solvent was ethyl acetate-butanone-methanoic acid-water(10∶1∶1∶1);The optimal sample quantities of the sample solution and the control solution were 4microlitres;TLC plate,temperature and relative humidity had no influence on the results.Conclusion:The method is convenient,reliable and accurate for the quality control of Bushen Yixin Tablet.
正在载入数据...
正在载入数据...
正在载入数据...
正在载入数据...
正在载入数据...
正在载入数据...
正在载入数据...
正在链接到云南高校图书馆文献保障联盟下载...
云南高校图书馆联盟文献共享服务平台 版权所有©
您的IP:18.221.185.110